简介
Nuclear magnetic resonsance (NMR) spectrocopy is the most powerful research tool used in chemistry today, but many chemists have yet to realize its true potential. Recent advances in NMR have led to a formidable array of new techniques - and acronyms - which leaves even the professionalspectroscopist bewildered. How, then, can chemists decide which approach will solve their particular structural or mechanistic problem?This book provides a non-mathematical, descriptive approach to modern NMR spectroscopy, taking examples from organic, inorganic, and biological chemistry. It also contains much practical advice about the acquisition and use of spectra. Starting from the simple 'one pulse' sequence, the textemploys a 'building block' approach to lead naturally to multiple pulse and two-dimensional NMR. Spectra of readily available compounds illustrate each technique. One- and two- dimensional methods are integrated in three chapters which show how to solve problems by making connections between spinsthrough bonds, through space, or through exchange. There are also chapters on spectrum editing and solids. The final chapter contains a case history which attempts to weave the many strands of the text into a coherent strategy.This second edition reflects the progress made by NMR in the past few years; there is a greater emphasis on inorganic nuclei; some two-colour spectra are used; the treatment of heteronuclear experiments has moved from direct to 'inverse' detection; many new examples and spectra have beenincluded; and the literature to early 1992 has been covered.An accompanying text, Modern NMR spectroscopy: A workbook of chemical problems, by Jeremy Sanders, Edwin Constable, and Brian Hunter, is available from OUP. Using a combination of worked examples and set problems, this workbook provides a practical guide to the accurate interpretation of NMRspectra, which will be of value to students and professional scientists alike.
目录
Introduction
The one-pulse experiment
Spin decoupling and difference spectroscopy
Multiple pulse experiments
The second dimension
Connections through bonds
Connections through space
Connections through chemical exchange
Editing
Solids
Sucrose octa-acetate: a case history
Symmetry, non-equivalence, and restricted rotation
Index
The one-pulse experiment
Spin decoupling and difference spectroscopy
Multiple pulse experiments
The second dimension
Connections through bonds
Connections through space
Connections through chemical exchange
Editing
Solids
Sucrose octa-acetate: a case history
Symmetry, non-equivalence, and restricted rotation
Index
- 名称
- 类型
- 大小
光盘服务联系方式: 020-38250260 客服QQ:4006604884
云图客服:
用户发送的提问,这种方式就需要有位在线客服来回答用户的问题,这种 就属于对话式的,问题是这种提问是否需要用户登录才能提问
Video Player
×
Audio Player
×
pdf Player
×